By Kash L. Mittal
This booklet records the court cases of the second one foreign Symposium on Adhesion size of movies and Coatings, held in Newark, NJ, October 25-27, 1999. This quantity includes 20 papers, that have all been conscientiously peer reviewed and certainly transformed ahead of inclusion. the subjects comprise: size and research of interface adhesion; relative adhesion dimension for skinny movie buildings; adhesion trying out of challenging coatings by means of numerous concepts; dimension of interfacial fracture strength in multifilm functions; laser brought about decohesion spectroscopy (LIDS) for measuring adhesion; pulsed laser method for evaluate of adhesion; blade adhesion try out; JKR adhesion try; coefficient of thermal growth size; and residual stresses in diamond motion pictures.
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Additional info for Adhesion Measurement of Films and Coatings, Volume 2
24. L. L. 1-13, VSP. Utrecht, The Netherlands (1995). 25. J. ), pp. 30-40, STP 640, ASTM, Philadelphia (1978). 26. J. Crocker, Rubber Chem. , 42, 30 (1968). 27. N. R. Hamed, Plast. Rubber Mater. , 17 (February 1978). 28. S. H. Kim, J. , 3, 175 (1989). 29. S. Kim and N. J. Solids Structures, 24, 417 (1988). 30. J. Kinloch, in: Fatigue of Advanced Materials. O. H. N. 439, Materials and Component Engineering Publications Ltd, Birmingham, UK (1991). 31. D. S. B. , 43, 1287 (1991). 32. P. K. L. 587, Marcel Dekker, New York (1996).
The cracked-off part is about 2pm thick. The brittle nature of the failure is characteristic to epoxies . The SEM micrograph series shown in Figure 21 is for the same sample but now from the epoxy side of the failure. Based on the height of the features seen in Figures 19 and 20 the fibers shown in Figure 21 are likely epoxy. Figure 21A shows a particularly good example of the varied character of the MELT locus of failure in this sample. Within an area of analysis of about 450ym x 375pm, several obviously different loci of failure Figure 20.
The SEM sample tilt angle was 30". P. Buchwalter Figure 21. SEM micrographs of the epoxy/low-k ILD/Si02/Si-wafer MELT locus of failure. A), B), and C) are of the same general area of the epoxy side of the failure. The SEM sample tilt angle was 30". can be detected. It is quite possible that at the onset of crack propagation a multitude of failure loci can be experienced simultaneously (recall that the onset of crack propagation is judged visually). If such varied paths are present as shown in Figure 21A, it is impossible to determine what the onset of crack propagation actually measures.